PET Aula 12-05-14 Grupo Misto
5799
Filename: C:\Program Files\Pyris\Data\Ricardo Gomes\PET_aula_12-05-14_grup o misto.ds8d Operator ID: Ricardo Gomes Sample ID: PET aula grupo misto Comment: 3 grupos Serial Number: 534N0100201 Data Collected: 12/5/2014 12:16:34 Sample Weight: 8.000 mg Display Weight: 8.000 Validation Validated: No By: Date: Calibration Information Filename: C:\Program Files\Pyris\Calibrations\17-01-14 ccs 20 Cmin-1 N2 20 mlmin-1pp.ds8c Date/Time: Initial Conditions Temperature: -20.00 °C Purge Gas: Purge Gas Rate: Baseline Filename: End Condition: Go To Load Total Points in Run: 173892 Method Steps: Pre-Run Actions Switch the Gas to Nitrogen at 20.0 ml/min Action occurs Immediately Start the Run Action occurs Immediately 1) Hold for 1.0 min at -20.00°C 2) Heat from -20.00°C to 280.00°C at 20.00°C/min 3) Hold for 1.0 min at 280.00°C 4) Cool from 280.00°C to -20.00°C at 20.00°C/min 5) Hold for 1.0 min at -20.00°C 6) Heat from -20.00°C to 280.00°C at 20.00°C/min 7) Hold for 1.0 min at 280.00°C 8) Cool from 280.00°C to -20.00°C at 20.00°C/min 9) Hold for 1.0 min at -20.00°C 10) Heat from -20.00°C to 280.00°C at 20.00°C/min 11) Hold for 1.0 min at 280.00°C 12) Cool from 280.00°C to -20.00°C at 50.00°C/min 13) Hold for 1.0 min at -20.00°C 14) Heat from -20.00°C to 280.00°C at 50.00°C/min 1) DSC 8500 Isothermal Time Unsubtracted Baseline Program Sample
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Transcript of PET Aula 12-05-14 Grupo Misto
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Filename: C:\Program Files\Pyris\Data\Ricardo Gomes\PET_aula_12-05-14_grupo misto.ds8d Operator ID: Ricardo Gomes Sample ID: PET aula grupo misto Comment: 3 grupos Serial Number: 534N0100201 Data Collected: 12/5/2014 12:16:34 Sample Weight: 8.000 mg Display Weight: 8.000 Validation Validated: No By: Date: Calibration Information Filename: C:\Program Files\Pyris\Calibrations\17-01-14 ccs 20 Cmin-1 N2 20 mlmin-1pp.ds8c Date/Time: Initial Conditions Temperature: -20.00 C Purge Gas: Purge Gas Rate: Baseline Filename: End Condition: Go To Load Total Points in Run: 173892 Method Steps: Pre-Run Actions Switch the Gas to Nitrogen at 20.0 ml/min
Action occurs Immediately Start the Run
Action occurs Immediately 1) Hold for 1.0 min at -20.00C 2) Heat from -20.00C to 280.00C at 20.00C/min 3) Hold for 1.0 min at 280.00C 4) Cool from 280.00C to -20.00C at 20.00C/min 5) Hold for 1.0 min at -20.00C 6) Heat from -20.00C to 280.00C at 20.00C/min 7) Hold for 1.0 min at 280.00C 8) Cool from 280.00C to -20.00C at 20.00C/min 9) Hold for 1.0 min at -20.00C 10) Heat from -20.00C to 280.00C at 20.00C/min 11) Hold for 1.0 min at 280.00C 12) Cool from 280.00C to -20.00C at 50.00C/min 13) Hold for 1.0 min at -20.00C 14) Heat from -20.00C to 280.00C at 50.00C/min 1) DSC 8500 Isothermal
Time Unsubtracted Baseline Program Sample
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Approx. Heat Flow Uncorrected Heat Flow Heat Flow Temperature Temperat
ure Gas Flow Calibration Heat Flow 0.000000 4.754853 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.754853 0.000500 4.758061 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.758061 0.001000 4.761482 0.000000 -20.000000 -19.7050
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00 0.000000 1.069179 4.764797 0.002000 4.768004 0.000000 -20.000000 -19.6960
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00 0.000000 1.069179 4.771212 0.003000 4.774419 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.774419 0.003500 4.777520 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.777520 0.004000 4.780727 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.780727 0.004500 4.783828 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.783828 0.005000 4.787035 0.000000 -20.000000 -19.6920
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00 0.000000 1.069179 4.802646 0.008000 4.805746 0.000000 -20.000000 -19.6880
00 0.000000 1.069179 4.805746 0.008500 4.808633 0.000000 -20.000000 -19.6880
00 0.000000 1.069179 4.808633 0.009000 4.811947 0.000000 -20.000000 -19.6880
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00 0.000000 1.069179 4.815048 0.010000 4.817828 0.000000 -20.000000 -19.6880
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00 0.000000 1.069179 4.820822 0.011000 4.823922 0.000000 -20.000000 -19.6880
00 0.000000 1.069179 4.823922 0.011500 4.827023 0.000000 -20.000000 -19.6880
00 0.000000 1.069179 4.827023 0.012000 4.829696 0.000000 -20.000000 -19.6880
00 0.000000 1.069179 4.829696 0.012500 4.832689 0.000000 -20.000000 -19.6880
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00 0.000000 1.069179 4.835683 0.013500 4.838463 0.000000 -20.000000 -19.6880
00 0.000000 1.069179 4.838463 0.014000 4.841671 0.000000 -20.000000 -19.6880
-
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00 0.000000 1.069179 4.847337 0.015500 4.850117 0.000000 -20.000000 -19.6960
00 0.000000 1.069179 4.850117 0.016000 4.853004 0.000000 -20.000000 -19.6960
00 0.000000 1.069179 4.853004 0.016500 4.855677 0.000000 -20.000000 -19.7000
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00 0.000000 1.069179 4.861343 0.018000 4.864230 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.864230 0.018500 4.867010 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.867010 0.019000 4.869790 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.869790 0.019500 4.872463 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.872463 0.020000 4.875350 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.875350 0.020500 4.877916 0.000000 -20.000000 -19.7050
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00 0.000000 1.069179 4.888928 0.023000 4.891387 0.000000 -20.000000 -19.7000
00 0.000000 1.069179 4.891387 0.023500 4.894167 0.000000 -20.000000 -19.7000
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00 0.000000 1.069179 4.896733 0.024500 4.899406 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.899406 0.025000 4.901972 0.000000 -20.000000 -19.7050
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00 0.000000 1.069179 4.907104 0.026500 4.909670 0.000000 -20.000000 -19.7000
00 0.000000 1.069179 4.909670 0.027000 4.912236 0.000000 -20.000000 -19.7000
00 0.000000 1.069179 4.912236 0.027500 4.914802 0.000000 -20.000000 -19.7050
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00 0.000000 1.069179 4.919721 0.029000 4.922073 0.000000 -20.000000 -19.7000
-
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00 0.000000 1.069179 4.932123 0.031500 4.934368 0.000000 -20.000000 -19.7050
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00 0.000000 1.069179 4.943670 0.034000 4.946022 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.946022 0.034500 4.948375 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.948375 0.035000 4.950620 0.000000 -20.000000 -19.7000
00 0.000000 1.069179 4.950620 0.035500 4.952758 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.952758 0.036000 4.955110 0.000000 -20.000000 -19.7050
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00 0.000000 1.069179 4.961846 0.038000 4.964092 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.964092 0.038500 4.966337 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 4.966337 0.039000 4.968368 0.000000 -20.000000 -19.7000
00 0.000000 1.069179 4.968368 0.039500 4.970507 0.000000 -20.000000 -19.6960
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00 0.000000 1.069179 4.972645 0.040500 4.974783 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.974783 0.041000 4.977029 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.977029 0.041500 4.979167 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.979167 0.042000 4.981305 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.981305 0.042500 4.983337 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.983337 0.043000 4.985368 0.000000 -20.000000 -19.6920
00 0.000000 1.069179 4.985368 0.043500 4.987507 0.000000 -20.000000 -19.6920
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-
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00 0.000000 1.069179 5.034444 0.056500 5.036154 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 5.036154 0.057000 5.037758 0.000000 -20.000000 -19.7050
00 0.000000 1.069179 5.037758 0.057500 5.039362 0.000000 -20.000000 -19.7050
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-
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-
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-
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